详细信息
文献类型:期刊文献
中文题名:ZnO晶体的水热法制备及性质研究
英文题名:Hydrothermal Synthesis and Characterization of ZnO Crystals
作者:刘鹏[1];张来苹[1];贾志凡[1];刘莉莉[1]
第一作者:刘鹏
机构:[1]新乡学院化学化工学院
第一机构:新乡学院化学化工学院
年份:2015
卷号:43
期号:17
起止页码:114-116
中文期刊名:广州化工
外文期刊名:Guangzhou Chemical Industry
语种:中文
中文关键词:氧化锌;水热法;表面活性剂;热温度
外文关键词:zinc oxide;hydrothermal method;surface active;hot temperature
摘要:采用水热法,以Zn(NO3)2·6H2O和Na OH为主要原料,加入表面活性剂,在高压反应釜中制得Zn O晶体。研究实验条件对Zn O晶体产率的影响;同时讨论了表面活性剂的种类及溶液p H对Zn O晶体产率的影响;利用红外光谱仪测量Zn O晶体的振动光谱,并利用粒度分析仪,研究表面活性剂的加入量对Zn O晶体分散性能的影响。实验表明,以Zn(NO3)2·6H2O和Na OH为主要原料,采用水热法,可以制得高纯度的Zn O晶体;表面活性剂聚乙二醇-600的加入量对Zn O晶体在水中的分散有重要的影响。
Chosing Zn(NO3)2·6H2O and NaOH as the main raw to prepare ZnO crystals in autoclavematerial under hydrothermal method, the influence of experimental conditions on ZnO crystal yield, the effects of the type of surfactant and the pH value were discussed. The infrared spectrometer of ZnO crystal and the size of ZnO particle were detected. From the study it was summerized that the amount of surfactant had important affection on the dispertion properties of ZnO crystals. The experimental results showed that the ZnO provided in this study can be obtained in high purity. The amount of surfactants, polyethylene glycol-600 dispersed in water had important influence on ZnO crystals.
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